본문 바로가기 주메뉴 바로가기

NMP GPC

We promise to support our clients with various organic/inorganic material R&Ds with utmost sincerity.

KOPTRI provides GPC (Gel Permeation Chromatography) service with NMP (N-Methyl-2-pyrrolidone).

NMP is a solvent that has even higher solubility than DMF and DMAc. If the polar polymer does not dissolve in NMP, it will be considered as a low solubility polymer or high chance of being crosslinked polymer, which would not be apt for GPC. For NMP, it is also effective to remove the polymer adsorption issue by adding LiBr or phosphoric acid as an additive. Especially for the cases below, if the polymer has many carboxylic acid (COOH) functional groups like polyamic acid, additives like phosphoric acid are useful. If you need help with analysis, please send us a request by submitting ‘Application Form’ under ‘Contact Us’ tab, and supervising researcher will aid you with a punctual and meticulous reply.

NMP GPC setup

※ Use left and right scroll for tables

Polymers MW range Temperature Standard Detector
Polyurethane
Polyamic acid
162 ~ 1,000,000 Da 50 ℃ PS
PMMA
PEG/PEO
RI

NMP GPC chromatogram of Polystyrene standards

NMP GPC chromatogram of Polyamic acid

  • Instrument : EcoSEC HLC-8320 GPC
  • Column (maker, model no.): TSKgel guardcolumn α + TSKgel α- M
  • Eluent : NMP + 0.06 N H3PO4
  • Temperature : 50 ℃
  • Flow rate : 0.5 mL/min
  • Injection volume, sample concentration : 50 ㎕, 3 mg/mL
  • Standard : Polystyrene
  • Detector : RI

Request a quote & inquiries

Request a Quote

If you fill out an application form by following the link below, we will send you a Quotation based on the information.

Inquiries

Inquiries

If you have questions on our available services, feel free to ask questions and we will send you a reply via e-mail.