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HT GPC

We promise to support our clients with various organic/inorganic material R&Ds with utmost sincerity.

KOPTRI professionally measures the molecular weight of crystalline polymers in polyolefin group that are insoluble in room temperatures by utilizing High Temperature-GPC (Gel Permeation Chromatography).

Eluent used to measure the molecular weight of polyolefin for high-temperature GPC is TCB(1,2,4-trichlorobenzene). Mechanical properties of Polyethylene or polypropylene will significantly affected on its molecular weight, molecular weight distribution, and branching, which requires quality control with GPC. Please give us a separate inquiry for ultra-high molecular weight polyethylene with a molecular weight of over a million. If semiconducting polymers such as polythiophene (aromatic conjugated polymer) does not dissolve in chloroform, we use TCB-GPC to measure the molecular weight. If you need help with analysis, please send us a request by submitting ‘Application Form’ under ‘Contact Us’ tab, and supervising researcher will aid you with a punctual and meticulous reply.

HT-GPC setup

※ Use left and right scroll for tables

Polymers MW range Temperature Standard Detector
LDPE
HDPE
LLDPE
PP
Polythiophene
Conjugated Polymer
500 ~
3,000,000 Da
160 ℃ TCB RI

TCB: 1,2,4-trichlorobenzene

HT-GPC Chromatogram of Polystyrene standards (TCB)

HT-GPC Chromatogram of Polyethylene (TCB)

  • Instrument : HLC-8321 GPC/HT
  • Column (maker, model no.): PLgel guard + 2 x PLgel mixed-B
  • Eluent : TCB (1,2,4-trichlorobenzene)
  • Temperature : 160 ℃
  • Flow rate : 1.0 mL/min
  • Injection volume, sample concentration : 300 ㎕, 1.5 mg/mL
  • Standard : Polystyrene
  • Detector : RI

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